积层多层板用UV油墨的合成研究

采用丙烯酸改性环氧树脂E－44的方法，合成了环氧丙烯酸酯预聚物，并将其用在UV光固化油墨的配方中。在树脂合成过程中，研究了反应温度，催化剂，阻聚剂等因素对合 产品的影响。通过L9(3^4)正交试验，得到了优化的工艺参数：反应温度为90℃，催化剂为N，N－二甲苯胺，用量1％；阻聚剂对苯二酚，用量0．5％，投料环氧树脂和丙烯酸的摩尔比为1：1．08。     

Investigation on the early and late stage phase-separation dynamics of poly(methyl methacrylate)/poly(α-methyl styrene-co-acrylonitrile) blends through rheological and scattering functions

The phase-separation behavior of poly(methyl methacrylate)/poly(α-methyl styrene-co-acrylonitrile) (PMMA/α-MSAN) blends with two different compositions was studied by time-resolved small angle light scattering (SALS) in the spinodal decomposition (SD) regime from 160 to 210 °C. The rheological function (WLF-like equation) was introduced into the processing of light scattering data. It was found that the WLF-like equation was applicable to describe the temperature dependence of apparent diffusion coefficient D_app and the relaxation time τ of normalized scattering intensity (I(t)−I(0))/(I_m−I(0)) at the early stage of SD, as well as the relaxation time τ of maximum scattering intensity I_m and characteristic scattering vector q_m with I_m at the late stage of SD for PMMA/α-MSAN blends with two different compositions. This is in consistence with the phase-separation behavior of PMMA/SAN reported in our previous paper.     

Electrochemical reaction of the SiMn/C composite for anode in lithium ion batteries

The SiMn-graphite composite powder was prepared by mechanical ball milling and its electrochemical performances were evaluated as the candidate anode materials for lithium ion batteries. It is found that the cyclic performance of the composite materials is improved significantly compared to SiMn alloy and pure silicon. The heat treatment of the electrodes is beneficial for enhancing the cyclic stabilities. The SiMn-20 wt.% graphite composite electrode after annealing at 200 °C has an initial reversible capacity of 463 mAh g⁻¹ and a charge-discharge efficiency of 70%. Moreover, the reversible capacity maintains 426 mAh g⁻¹ after 30 cycles with a coulomb efficiency of over 97%. The phase structure and morphology of the composite were analyzed by X-ray diffraction (XRD) and scanning electron microscopy. The lithiation/delithiation behavior was investigated by electrochemical impedance spectroscopy (EIS) and cyclic voltammetry. The composite materials appear to be promising candidates as negative electrodes for lithium rechargeable batteries.     

日本太空军事化的影响及对我国的警示

日本太空军事化已早有打算,其军事利用太空已达到较高水平。日本太空军事化深层战略目的是为今后太空战作准备,而美国却对日本太空军事化采取扶持态度。日本太空军事化给全世界尤其是亚洲国家造成极其恶劣影响,我们需引起高度的重视。     

刑法的本质与罪刑法定原则

罪刑法定原则是现代刑法所确立的一项重要原则,其对人权保障具有里程碑意义.在我国,要真正贯彻好罪刑法定原则,必须对"刑法"的本质进行科学理解和把握,真正实现刑法的目的和任务.     

《小镇畸人》中的词汇衔接分析

词汇衔接是英语语篇中重要的衔接手段之一.以Halliday等语言学家的衔接理论为基础,分析了舍伍德·安德森的<小镇畸人>中词汇衔接的分类和作用,探讨了各种词汇衔接机制在语篇连贯构建中的独特意义.     

边坡锚固工程分析中的水平条分法

对目前中国规范推荐用于边坡加固计算的垂直条分传递系数法进行研究,发现将该方法用于边坡锚固受力分析时,不仅存在垂直条块与加固结构体（锚杆和锚索）相互交叉,而且计算得出的锚固力与加固体的实际锚固力存在偏差等缺陷。在相关资料提出的、用于加筋土稳定性分析的水平条分法基础上,结合边坡锚固工程的特点,将该水平条分法做进一步拓展,使其能适用于锚杆和锚索等边坡锚固工程的稳定性计算,并通过工程实例对拓展后的水平条分法进行了验证。     

美国《1990年建筑作品版权保护法》评述

在1990年12月以前,建筑作品是作为绘画、图形和雕塑作品获得版权保护的.但是建筑本身被认为是一种实用物品,因而不受版权的保护.然而在1989年3月1日,美国加入《伯尔尼公约》.为了履行公约义务,美国国会通过了《1990年建筑作品版权保护法》(简称AWCPA),对《1976年版权法》进行了相应的修正,建筑作品作为独立的一类作品受版权法的保护,拓宽了建筑作品的保护范围,对建筑作品侵权的认定标准也发生变化.     

Crystallization and conductivity mechanism of ITO films on different substrates deposited with different substrate temperatures

ITO thin films were grown on PC(polycarbonate), PMMA(polymethyl methacrylate) and glass substrates by r.f. magnetron sputtering. The electrical, structural and chemical characteristics of ITO films were analyzed by the Hall Technique, X-ray diffraction, and X-ray photoelectron spectroscopy. XPS studies suggest that all the ITO films consist of crystalline and amorphous phases. The degree of crystallinity increases from less than 45% to more than 90% when the substrate temperature increases from 80 to 300 ℃. The In and Sn exist in the chemical state of In3+ and Sn4+, respectively, independent of substrate type and temperature. The enrichment of Sn on surface and In in body of ITO films are also revealed. And, the oxygen deficient regions exist both in surface layer and film body. For ITO films deposited under 180 ℃ , the carrier concentration are mainly provided by oxygen vacancies, and the dominant electron carrier scattering mechanism is grain boundary scattering between the crystal and the amorphous grain. For ITO films deposited over 180 ℃, the carrier concentration are provided by tin doping, and the dominant scattering mechanism transforms from grain boundary scattering between the crystal grains to ionized impurity scattering with increasing deposition temperature.     

带钢轧机导卫设备的改进及自动控制

为了满足现代化的生产需求,采用双丝杠传动,解决了带钢轧机导卫设备的主传动机构导卫刚度和可调性差问题,实现了导卫前后的同步运动和双导向,同步导向误差率低于1％;液压移出装置,解决了在线检修影响生产和不能整体移入移出的问题,提高了设备维修的效率;水雾除尘装置,增加了导卫降尘的功能,消除了烟尘对环境的污染,降尘量达到90％;同时设计了自动化控制系统,生产效率提高60％。